预试环中H_2及掺杂甲烷的辉光放电清洗

本文给出了在预试环中产生和维持辉光放电的基本参数、氢气(H_2)及氢气掺杂甲烷(H_2/CH_4)辉光放电清洗过程中的质谱分析结果以及氢气辉光放电清洗处理后的样品表面SIMS(二次离子质谱)结果,并进行了讨论。     

Underwater and water-assisted laser processing: Part 1—general features, steam cleaning and shock processing

Water is always present in laser processing in air: as vapor, condensate or adsorbate. Water is the working environment in underwater processing—but it can also be added on purpose to gain better results: to avoid redeposition of debris, to cool the material, to increase plasma pressure or to conduct light. Water can also act as a chemical reagent. The first part of the article will review the advantages and disadvantages of laser processing in the presence of water, light transmission by water, and the two most mature methods of water-assisted laser processing: steam cleaning and shock processing.     

Cyclin A-Cdk2 Phosphorylates BH3 only Protein Bad in vitro and in vivo

Increasing evidence suggests that Cyclin A-Cdk2 activity is required in the apoptosis process induced by various stimuli. To determine a specific substrate of Cyclin A-Cdk2 for apoptosis, in this study, we carried out anin vitro kinase assay using immunoprecipitated complex Cyclin A-Cdk2 as an enzyme source, and recombinant protein GST-Bad as a substrate. Our study showed that Bad was clearly phosphorylated by Cyclin A-Cdk2 in vitro. To examine whether protein Bad can also be phosphorylated by Cyclin A-Cdk2 kinase in vivo, we transiently overexpressed protein Bad with Cyclin A or Cdk2-dn, a dominant negative version of Cdk2, in Hela cells and determined the phosphorylation status of protein Bad. The test showed that protein Bad was clearly phosphorylated in Cyclin A overexpressed cells,but not in Cdk2-dn or mock transfectent. Moreover, etoposide also caused the phosphorylation of endogenetic Bad. In conclusion, here we provide first time evidence that protein Bad can be a substrate of Cyclin A-Cdk2 apoptosis for in vitro and in vivo.     

Ultraviolet laser removal of small metallic particles from silicon wafers

Laser removal of small 1 μm sized copper, gold and tungsten particles from silicon wafer surfaces was carried out using ultraviolet radiation at 266 nm generated by Nd:YAG harmonic generation. Successful removal of both copper and gold particles from the surface was achieved whereas tungsten particles proved to be difficult to remove. The cleaning efficiency was increased with an increase of laser fluence. The optimum processing window for safe cleaning of the surface without any substrate damage was determined by measuring the damage threshold laser fluence on the silicon substrate and the required fluence for complete removal of the particles. The different cleaning efficiencies with particle type are discussed by considering the adhesion force of the particle on the surface and the laser-induced cleaning force for the three different particles.     

井下多股淹没射流水力清岩能力分析

研究石油钻井井下射流的水力清岩能力对钻井业有重要意义。本文借助于预处理方法和多块网格对接技术由计算机数值模拟了形状复杂的钻井PDC钻头井底下的多股淹没射流流场。为体现井底有岩屑时射流场对其的清洗作用。文中借助河流泥沙运动理论，分析了岩屑在井下的受力与运动以考虑固相的作用。因岩屑主要为推移运动。在井底除环空外的大部分地方可简化视为二维运动。提出了钻头井底水力清岩能力的体现参数-水力挟岩力。并通过数值模拟显示了井下流场，描述了转速，射流流量，喷嘴面积，射流雷诺数及井下过流空间等流场控制参数对井底水力清岩能力的不同影响，指出相关水力参数在射流时的优化方向。为复杂的井底流场控制和钻头的合理设计做探索基础。     

Photocatalytically Renewable Micro‐electrochemical Sensor for Real‐Time Monitoring of Cells

Electrode fouling and passivation is a substantial and inevitable limitation in electrochemical biosensing, and it is a great challenge to efficiently remove the contaminant without changing the surface structure and electrochemical performance. Herein, we propose a versatile and efficient strategy based on photocatalytic cleaning to construct renewable electrochemical sensors for cell analysis. This kind of sensor was fabricated by controllable assembly of reduced graphene oxide (RGO) and TiO₂ to form a sandwiching RGO@TiO₂ structure, followed by deposition of Au nanoparticles (NPs) onto the RGO shell. The Au NPs‐RGO composite shell provides high electrochemical performance. Meanwhile, the encapsulated TiO₂ ensures an excellent photocatalytic cleaning property. Application of this renewable microsensor for detection of nitric oxide (NO) release from cells demonstrates the great potential of this strategy in electrode regeneration and biosensing.     

The superhydrophobicity of polymer surfaces: Recent developments

Superhydrophobicity is the extreme water repellence of highly textured surfaces. The field of superhydrophobicity research has reached a stage where huge numbers of candidate treatments have been proposed and jumps have been made in theoretically describing them. There now seems to be a move to more practical concerns and to considering the demands of individual applications instead of more general cases. With these developments, polymeric surfaces with their huge variety of properties have come to the fore and are fast becoming the material of choice for designing, developing, and producing superhydrophobic surfaces. © 2011 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 49: 1203–1217, 2011     

Advanced Materials in Cultural Heritage Conservation

Cultural Heritage is a crucial socioeconomic resource; yet, recurring degradation processes endanger its preservation. Serendipitous approaches in restoration practice need to be replaced by systematically addressing conservation issues through the development of advanced materials for the preservation of the artifacts. In the last few decades, materials and colloid science have provided valid solutions to counteract degradation, and we report here the main highlights in the formulation and application of materials and methodologies for the cleaning, protection and consolidation of works of art. Several types of artifacts are addressed, from murals to canvas paintings, metal objects, and paper artworks, comprising both classic and modern/contemporary art. Systems, such as nanoparticles, gels, nanostructured cleaning fluids, composites, and other functional materials, are reviewed. Future perspectives are also commented, outlining open issues and trends in this challenging and exciting field.     

NEA GaAs光电阴极激活工艺研究

本文报道了 GaAs 反射式光电阴极的激活工艺过程和结果.通过实验确定了 GaAs表面的热清洁温度,利用钼丝热辐射加热方法达到了比较理想的清洁效果,采用铯分子源和高纯氧作氧源获得了高于1000μA/1m 的激活积分灵敏度.     

Analytical modeling of loss characteristics of a polymer arrayed waveguide grating multiplexer

Theoretical analysis is performed for the loss characteristics of a polymer arrayed waveguide grating (AWG) multiplexer around the central wavelength of 1.55 μm with the wavelength spacing of 1.6 nm. The total loss of the device includes the diffraction loss in the input and output (I/O) slab waveguides, bent loss caused by the AWG and I/O channels, leakage loss resulted from the high refractive index substrate, and propagation loss due to the absorption and scattering of the materials of the device. The effects of some structural parameters on the loss characteristics are investigated and discussed. The computed results show that when we select the core thickness as 4 μm, core width as 6 μm, pitch of adjacent waveguides as 15.5 μm, diffraction order as 50, the number of the arrayed waveguides as 91, that of the I/O channels as 17, confined layer thickness between the core and the substrate as 10 μm, distance between the focal point and the origin as 5500 μm, and central angle between the central waveguide and the x-axis (i.e. the vertical of the symmetrical line of the device) as 60°, the total loss of the device can be dropped to the range 3.79–7.93 dB.